2-脱氧-2-苯二酰亚胺-1,3,4,6-四-氧-乙酰-β-D-吡喃葡萄糖合成路线 (共 55 条)
反应条件
1: sodium hydroxide / water / 20 °C 2: pyridine / 0 - 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 15 p. 3019 - 3032
反应条件
4-(N,N-dimethlyamino)pyridine; acetic anhydride in dichloromethane Yield given;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 63, # 4 p. 577 - 589
反应条件
1: aq. NaHCO3 / acetone / 3 h / 50 °C 2: 2.00 g / pyridine / 16 h / 50 °C View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 68, # 7 p. 1264 - 1274
反应条件
1: 4-DMAP / CH2Cl2 / Ambient temperature 2: 4-DMAP, Ac2O / CH2Cl2 View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 63, # 4 p. 577 - 589
反应条件
1.1: sodium methylate / methanol / 3 h / 20 °C / |Inert atmosphere 1.2: 6 h / 20 °C / |Inert atmosphere 2.1: pyridine / 12 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 14 p. 4157 - 4161
反应条件
pyridine T=20°C; 48 h;
参考文献
Chemistry - A European Journal, , vol. 12, # 25 p. 6478 - 6485
反应条件
1.1: sodium methylate / methanol / Inert atmosphere 1.2: Inert atmosphere 2.1: pyridine; 4-(N,N-dimethlyamino)pyridine / Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 47 p. 11167 - 11171
反应条件
pyridine T=50°C; 16 h;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 68, # 7 p. 1264 - 1274
反应条件
pyridine; triethylamine 1.) MeOH, water, 1 h, 50 deg C; 2.) 1 h, 100 deg C; Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 125, p. 237 - 246
反应条件
pyridine; acetic anhydride 1.) 90 deg C, 90 min, 2.) 90 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Australian Journal of Chemistry, , vol. 47, # 3 p. 433 - 440