2-脱氧-2-苯二酰亚胺-1,3,4,6-四-氧-乙酰-β-D-吡喃葡萄糖合成路线 (共 55 条)
反应条件
triethylamine 1.) pyridine, 75 min, 2.) 90-95 deg C, 10 min; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 53, # 12 p. 4159 - 4178
反应条件
1: triethylamine / 50 °C 2: pyridine / 16 h / 20 °C View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 86, # 10 p. 1112 - 1114
参考文献
Yakugaku Zasshi, , vol. 77, p. 726,730
Chem.Abstr., , p. 17763
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate research, , vol. 162, # 2 p. 227 - 235
参考文献
Journal of Organic Chemistry, , vol. 19, p. 1793,1798
反应条件
1: 76.8 percent / SnCl4 / CH2Cl2 / 15 h 2: BuNH2 / ethanol / Heating 3: 250 mg / pyridine / 25 °C View Scheme
参考文献
Ats, Sandor-Csaba; Lehmann, Jochen; Petry, Stefan
Carbohydrate Research, 1992 , vol. 233, p. 125 - 139
反应条件
dichloromethoxy methane; boron trifluoride diethyl etherate in chloroform T=65°C; 3 h; Inert atmosphere;
参考文献
Bednarczyk, Dorota; Walczewska, Agata; Grzywacz, Daria; Sikorski, Artur; Liberek, Beata; Myszka, Henryk
Carbohydrate Research, 2013 , vol. 367, p. 10 - 17
反应条件
bismuth(III) chloride; thionyl chloride in dichloromethane T=20°C; 12 h; Reagent/catalystTime; Overall yield = 86 percent;
参考文献
Cao, Zhiling; Liu, Wenjie; Qu, Yingying; Yao, Guowei; Gao, Dachao; Liu, Weiwei
Journal of Chemical Research, 2013 , vol. 37, # 8 p. 467 - 469
反应条件
tin(IV) chloride in 1,2-dichloro-ethane T=20°C; 15 h;
参考文献
Ogawa, Tomoya; Nakabayashi, Satoru; Sasajima, Kikuo
Carbohydrate Research, 1981 , vol. 95, p. 308 - 312
反应条件
boron trifluoride diethyl etherate in dichloromethane T=0 - 20°C; 4 h;
参考文献
Pozsgay; Jennings
Carbohydrate research, 1988 , vol. 179, p. 61 - 75