in neat (no solvent) react. (FXeOXeFXeF)(AsF6) with NO2F at -50°C for 5 h; excess NO2F was removed in vacuo at -110°C, SO2ClF was condensed at -196°C, soln. was warmed to -30°C, decanted and evapd. in vacuo;
参考文献
Moran, Matthew D.; Brock, David S.; Mercier, Helene P. A.; Schrobilgen, Gary J.
Journal of the American Chemical Society, 2010 , vol. 132, # 39 p. 13823 - 13839
in neat (no solvent) react. (FXeOXeFXeF)(AsF6) with NO2F at -50°C for 5 h; excess NO2F was removed in vacuo at -110°C, SO2ClF was condensed at -196°C, soln. was warmed to -30°C, decanted and evapd. in vacuo;
参考文献
Moran, Matthew D.; Brock, David S.; Mercier, Helene P. A.; Schrobilgen, Gary J.
Journal of the American Chemical Society, 2010 , vol. 132, # 39 p. 13823 - 13839
Moissan; Lebeau
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 140, p. 1573 - 1621
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Gmelin Handbook: F: MVol., 22, page 50 - 51
