3-甲基-4-甲氧基苯乙酮合成路线 （共 26 条）
反应条件
pyridine hydrochloride
参考文献
Bulletin de la Societe Chimique de France, , p. 611 - 615
反应条件
sodium hydroxide; potassium chloride; potassium hexacyanoferrate(III) in methanol; water T=30°C; further temperature; activation energy; Thermodynamic dataKinetics;
参考文献
Journal of the Indian Chemical Society, , vol. 63, p. 1055 - 1059
参考文献
Journal of the American Chemical Society, , vol. 53, p. 3184
反应条件
1: With 3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; Baeyer-Villiger oxidation reaction; 14 h;
2: With sodium hydroxide in methanol
T=20°C; 5 h; Further stages.;
参考文献
Roy, Amalesh; Biswas, Bidyut; Sen, Prabir K.; Venkateswaran, Ramanathapuram V.
Tetrahedron Letters, 2007 , vol. 48, # 39 p. 6933 - 6936
反应条件
(i) PCl5, CHCl3, (ii) NaNH2, liq. NH3, THF; Multistep reaction;
参考文献
Tani,H. et al.
Bulletin of the Chemical Society of Japan, 1964 , vol. 37, p. 919 - 923
反应条件
1: NH4OAc, AcOH / benzene / Heating
2: Al-Hg, H2O
3: (i) aq. HCl, (ii) aq. KOH, diethylene glycol
4: polyphosphoric acid / Heating
5: (i) N2H4*H2O, diethylene glycol, (ii) aq. HCl
View Scheme
参考文献
Das,T.K. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1977 , p. 1287 - 1295
