Nicolardot, p.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1908 , vol. 147, p. 1304 - 1306
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Gmelin Handbook: S: MVol.B3, 113, page 1773 - 1775
in neat (no solvent) S2Cl2 and crystalline Si in a Cl2 stream at vigorous red heat;; isolation by distillation, purification by recrystallization in CCl4;;
in 1,1,2,2-tetrachloroethylene; chloroform refluxing of soln. of educts (8 h), distn. of solvent, warming of residue at 100-150°C and 20-40 Torr (2 h); sublimation, recrystn. (twice) from chlorobenzene;
参考文献
Journal of the American Chemical Society, , vol. 80, p. 2775 - 2778
