in melt exchange reaction (KCl/NaCl melt, 1073 K);
参考文献
Shkol'nikov, S. N.; Tolpin, E. S.; Zatitskii, B. E.
Journal of Applied Chemistry USSR (English Translation), 1982 , vol. 55, p. 286 - 289
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1982 , vol. 55, p. 319 - 322
→
反应条件
in neat (no solvent, solid phase) byproducts: LiCl, N2; Sonication; grinding in agate mortar; sealing in glass ampoule under vac.; sonicating (ultrasonic gun), 10 min; heating, 400°C, 5-10 min; sublimation of LiCl onto reactor walls; cooling to room temp.; open of ampoule under N2; trituration with THF, 10h; pptn.; washing with water or THF;
参考文献
Fitzmaurice, Jonathan C.; Hector, Andrew L.; Parkin, Ivan P.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1993 , # 16 p. 2435 - 2438
