Wolinsky, L.; Tieckelmann, H.; Post, H. W.
Journal of Organic Chemistry, 1951 , vol. 16, p. 395 - 398
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.C, 144, page 393 - 397
Petrov, A. D.; Tsernysev, E. A.
Doklady Akademii Nauk SSSR, 1952 , vol. 86, p. 737 - 740
C. A., 1953 , p. 8010
Full Text Show Details
Gmelin Handbook: Si: MVol.C, 36, page 111 - 115
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in N-dodecane 0.5 h; Inert atmosphere; Product distribution / selectivity;
参考文献
KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY; YOO, Bok Ryul; HAN, Joon Soo; YOO, Jang Hyun
Patent: WO2011/81277 A2, 2011 ;
Location in patent: Page/Page column 16-18 ;
antimony(V) pentachloride in neat (no solvent) byproducts: SiH4, HCl; at room temp. for 3 h; products distd. through two traps (-93°C, toluene slush, -130°C pentane slush), the second trap containing HSiF3 was isolated, evacuated for 30 min at -130°C (1.0 torr) to remove SiH4, HCl;
antimony pentachloride in neat (no solvent) byproducts: H2; conversion of 2.093g SiHCl3 with 0.5g SbF3 in presence of 0.2ml SbCl5 at 10-15 °C for a period of 3 hours;;
参考文献
Emeleus, H. J.; Maddock, A. G.
Journal of the Chemical Society, 1944 , p. 293 - 296
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.B, 233, page 635 - 638
