反应条件
NEt3 in pentane byproducts: HNEt3Cl; absence of air and moisture; slow addn. of 1 equiv. NEt3 to mixt. of 1 equiv. of HSiCl3 and 0.9 equiv. of Me3GeCl, stirring (room temp., 20 h); filtration, evapn. at 0°C, distn. (31°C, 3.5 mbar); elem. anal.;
参考文献
Hinchley, Sarah L.; McLachlan, Lorna J.; Robertson, Heather E.; Rankin, David W.H.; Seppaelae, Emma; du Mont, Wolf-Walther
Inorganica Chimica Acta, 2007 , vol. 360, # 4 p. 1323 - 1331
