hydrogenchloride; lithium aluminium tetrahydride in benzene Kinetics; introduction of HCl gas into a soln. of HSi(SiCl3)3 and a very few trimethylamine, at room temp.; detection by Raman and (1)H-NMR;
in gas Kinetics; Irradiation (UV/VIS); infrared laser irrdn. of SiH4-HCl mixt. in pressure range of 28-60 torrand in temp. range of 295-414 K; analyzed by mass spectrometry;
参考文献
Journal of the American Chemical Society, , vol. 106, # 25 p. 7761 - 7765
hydrogenchloride in tetrahydrofuran; diethyl ether addn. of soln. of BrSiCl3 in THF to soln. of org.compd. in THF (-78°C), stirring (2 h, -78°C), addn. of HCl in ether; not isolated; (1)H-NMR spectrometry;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 572, p. 186 - 191
hydrogenchloride; lithium aluminium tetrahydride in chloroform Kinetics; introduction of HCl gas into a soln. of Si5Cl12 and trimethylammonium bromide or chloride (equimolar amts.), at room temp.; detection by Raman and (1)H-NMR;
