反应条件
ethanol in 1,4-dioxane byproducts: CH3Cl, HCl; addn. of suspn. of (Cl3PNPCl3)PCl6 in dioxane to ethanol in dioxane (molar ratio 1:3) dropwise during 1 h at ambient temp.; not isolated; (31)P-NMR spectroscopic monitoring;
参考文献
Phosphorus, Sulfur, and Silicon and the Related Elements, , vol. 63, p. 19 - 32