Lehmstedt; Schrader
Chemische Berichte, 1937 , vol. 70, p. 838,845
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Albert; Ritchie
Journal of the Society of Chemical Industry, London, 1941 , vol. 60, p. 121,122
Organic Syntheses, 1942 , vol. 22, p. 6
in acetonitrile byproducts: KCl, HCl; a mixt. of KHF2 and POCl3 (equal amts.) in MeCN was stirred for 24 h at room temp.;; the solvent was distd. off, the solid residue agitated with EtOH, KPF6 pptd. by addn. of ether; after filtration, the filtrate was evapd. to yield KPO2F2; elem. anal.;
参考文献
Kalbandkeri, R. G.; Padma, D. K.; Vasudeva Murthy, A. R.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1984 , vol. 23, p. 990 - 991
