in neat (no solvent) equimolar ratio; placed in ampul, sealed under vac.; carefully mixed; heated at 250°C; SbCl3 sublimed and crystd. in cooled part of ampul; chem. anal.; DTA; XRD;
参考文献
Inorganic Materials (Transl. of Neorg. Mater.), , vol. 19, p. 1532 - 1534
Izvestiya Akademii Nauk SSSR, Neorganicheskie Materialy, , vol. 19, p. 1733 - 1735
in dichloromethane byproducts: SO2, N2; stirring mixt. of Te-compd. and SbCl5 (molar ratio 2.1:1.5) in abs. CH2Cl2 at -80°C in a sealed tube (12 h); filtration of pptn. in absence of air and moisture, washing (CH2Cl2), concn. of combined filtrates by removal of solvent in vac. to half of vol., crystn. after few weeks;
参考文献
Haas, A.; Pohl, R.
European Journal of Solid State and Inorganic Chemistry, 1992 , vol. 29, p. 791 - 798
