反应条件
sodium hydroxide; isopropyl alcohol in water other Radiation; NaOH soln. dropping into Sb-salt soln. (hydrolysis prevention, PVA or SDS as surfactant, i-PrOH as scavenger of OH radicals ), bubbling with N2 for 1 h, irradiation in a field of 70000 Ci (60)Co γ-ray source, 8.82E+4 Gy radiation dose, pptn.; ppt. filtration off, washing (water, alcohol), vac. drying at 60°C; optical microscopy;
参考文献
Liu; Qian; Wang; Zhang
Materials Research Bulletin, 1996 , vol. 31, # 8 p. 973 - 977
