Dollimore, D.; Long, L. H.
Journal of the Chemical Society, 1953 , p. 3906 - 3910
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Gmelin Handbook: B: B-Verb.9, 6.2.2, page 269 - 280
1,5-diazo-bicyclo{4.3.0}5-nonene in tetrahydrofuran
exothermic react.; evapn. of mixt.; intermediates dissolved in tetraglyme and treated with 1,5-diazo-bicyclo(4.3.9)5-nonene; vac. distn. to receiver cooled by dry ice;
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Ashe; III
Journal of the American Chemical Society, 1971 , vol. 93, p. 6690
in diethyl ether
treating with water, concn., adding ethanol;
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Glushkova, V. P.; Talalaeva, T. V.; Razmanova, Z. P.; Zhdanov, G. S.; Kocheshkov, K. A.
Sb. Statei Obshch. Khim. Akad. Nauk SSSR, 1953 , vol. 2, p. 992 - 996
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Gmelin Handbook: Sb: Org.Comp.1, 1.1.1.1.7, page 87 - 96
n-butyllithium in tetrahydrofuran; diethyl ether; hexane
byproducts: LiBr; A soln. of o-C6H4Br(NMe2) in Et2O was added dropwise to n-BuLi in hexane at 0°C, after 1 h a soln. of SbCl3 in THF was added, the mixt. was refluxed for 30 min (N2 atm.);; hydrolysis the organic layer was sepd., dried and evapd., recrystd. from ethanol and acetone; elem. anal.;;
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Levason, William; Sheikh, Baharuddin
Journal of Organometallic Chemistry, 1981 , vol. 209, # 2 p. 161 - 168
