反应条件
CS2 in carbon disulfide TaCl5 was placed in ampoule under a stream of N2, ampoule was evacuated, left to pump for 0.5 h, Sb2S3 was pumped at 200°C overnight, CS2 was distilled into ampoule, cooled to liq. N2 temp., solvent was added, stirred at room temp. for 3 d; ampoule quickly opened under N2, filtered on vac. line, ppt. was washedwith CS2, pumped for 24 h; elem. anal.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 845 - 848
