反应条件
in water stirred at 60°C for 6 h with a large excess of benzonitrile, pumped to dryness; extd. (CH2Cl2), soln. dried (Na2SO4, 2 h), filtered, taked to dryness (reduced pressure), treated with hot benzene, filtered, residue washed (petroleum ether), dried under vacuo, the same procedure for the benzene soln. gave the trans-isomer; elem.anal.;
参考文献
Inorganica Chimica Acta, , vol. 201, p. 15 - 22
