in ethanol; water
formation on mixing of the aq. soln. of K2(PtCl4) with excess alc. soln. of l-1,2-diamino-1,2-diphenylethane; pptn. after some days;; washing with H2O, alcohol and ether;;
参考文献
Lifschitz, I.; Bos, J. G.
Rec. Trav. chim., 1940 , vol. 59, p. 407 - 422
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Gmelin Handbook: Pt: MVol.D, 122, page 278 - 280
in methanol; water
a bit more than 2 equiv. of N-compd. in MeOH was added to Pt-compd. soln. in H2O, stirring without protection from light at room temp. for 24 h; ppt. was filtered off, dried over P2O5, elem. anal.;
in ethanol; water
slow addn. of aq. K2PtCl4 to stirred soln. of 2 equiv. of ligand in hot alcohol, heating (steam bath, 10 min; pptn.); hot filtration, washing (water, alcohol), drying (vac., over silica gel); elem. anal.;
in ethanol; water
slow addn. of aq. K2PtCl4 to stirred soln. of 2 equiv. of ligand in hot alcohol, heating (steam bath, 10 min; pptn.); hot filtration, washing (water, alcohol), drying (vac., over silica gel); elem. anal.;
in ethanol; water
slow addn. of aq. K2PtCl4 to stirred soln. of 2 equiv. of ligand in hot alcohol, heating (steam bath, 10 min; pptn.); hot filtration, washing (water, alcohol), drying (vac., over silica gel); elem. anal.;
in ethanol; water
slow addn. of aq. K2PtCl4 to stirred soln. of 2 equiv. of ligand in hot alcohol, heating (steam bath, 10 min; pptn.); hot filtration, washing (water, alcohol), drying (vac., over silica gel); elem. anal.;
in ethanol; water
slow addn. of aq. K2PtCl4 to stirred soln. of 2 equiv. of ligand in hot alcohol, heating (steam bath, 10 min; pptn.); hot filtration, washing (water, alcohol), drying (vac., over silica gel); elem. anal.;
Banerjee, Swagata; Kitchen, Jonathan A.; Bright, Sandra A.; O'Brien, John E.; Williams, D. Clive; Kelly, John M.; Gunnlaugsson, Thorfinnur
Chemical Communications, 2013 , vol. 49, # 76 p. 8522 - 8524
