反应条件
potassium permanganate; ammonia; sodium sulfite in water heating of aq. soln. of Pt-compd. to 70-80°C, addn. of soln. of ammonia with stirring, heating till dissolution of precipitate, addn. of Na2SO3, further heating for 30 min, cooling to 30-40°C, acidifying with H2SO4, titration with KMnO4; addn. of HCl, concn., cooling, filtn., washing with water, ethanol, ether, elem. anal.;
参考文献
Gel'fman, M. I.; Kovalevich, O. V.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1992 , vol. 37, p. 912 - 915
Zhurnal Neorganicheskoi Khimii, 1992 , vol. 37, p. 1785 - 1789
