in neat (no solvent) passing dry Cl2 through a glass tube, filled with Ca-silicide and heated by a electric spiral at 150-250 °C for about 12-14 days, further products;; fractional distillation;;
参考文献
Si: MVol.B, 242, page 657 - 659
Booth, H. S., Inorganic syntheses, Bd. 1, New York-London 1939, S. 42
in gas Irradiation (UV/VIS); on photolysis (>= 300nm) of a Cl2-SiHCl3-N2-mixture (0.3 Torr Cl2 and 0.3Torr SiCl4 in 700 Torr N2);; not isolated, monitoring of react. by IR;;
参考文献
Journal of Physical Chemistry, , vol. 89, # 17 p. 3725 - 3729
