反应条件
in neat (no solvent) byproducts: (t-C4H9)(i-C3H7)PSiCl3, (t-C4H9)(i-C3H7)PSi2Cl5, (t-C4H9)(-i-C3H7)PH; N2 atmosphere, addn. of Si2Cl6 to ice-cooled stannyl compound, warming to room temp., 20 min; other reaction time; (29)Si- and (31)P-NMR-monitoring;
