反应条件
byproducts: H2, CH4, CH3SiCl3; vaporization of Cl2Si(CH3)2 from a carburetor, pyrolysis in purified Ar (4percent DMS in 96percent Ar, 700-1100°C, contact time ca. 1 min, pressure of 1 atm, tubular reactor heated in a furnace), vac. deposition of solid powder; products not isolated, detn. of gaseous products by chromy. (equil. concentrations of gases at various temps.), detn. of solid products by IR, pyrolysis reacts., AFNOR refactory analysis (after oxidn. of solid material at 750°C, 30 min);
参考文献
Journal of the American Ceramic Society, , vol. 73, # 3 p. 607 - 614
