反应条件
triethylamine in water; diethylene glycol byproducts: NaCl, H2; NaBH4 in diglyme heated to 105°C, soln. SiCl4 in diglyme added dropwise, mixt. filtered, filtrate stripped to oil, dissolved in water and Me4NCl added; ppt. filtered and recrystd. from acetone/water;
参考文献
Dunks, Gary B.; Barker, Kathryn; Hedaya, Eddie; Hefner, Catherine; Palmer-Ordonez, Kathy; Remec, Peter
Inorganic Chemistry, 1981 , vol. 20, p. 1692 - 1697
