antimony pentachloride in neat (no solvent) isolation by fractional distillation;;
参考文献
Booth, H. S.; Swinehart, C. F.
Journal of the American Chemical Society, 1935 , vol. 57, p. 1333 - 1342
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Gmelin Handbook: Si: MVol.B, 262, page 708 - 710
in gas passing a SiCl4 containing SiF4 vapor stream through a glass tube, heated up to 600 °C;; condensation at -30 °C and separation by fractionation;;