in neat (no solvent, gas phase) mixt. of SiCl4 and PhCH2OSiCl3 are passed through empty quartz tube heated to 620°C (20-30 sec stayed in reaction zone, gas phase reaction), further product: Cl3SiOSiCl2OSiCl3 (10.5percent);
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 57, p. 1142 - 1146
Zhurnal Obshchei Khimii, , vol. 57, p. 1275 - 1280