Journal of the American Chemical Society, , vol. 75, p. 3762 - 3765
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反应条件
800-1100 K; tensimetry;
参考文献
Baklanova, N. I.; Kulyukin, V. N.
Inorganic Materials (Transl. of Neorg. Mater.), 1990 , vol. 26, p. 77 - 80
Izvestiya Akademii Nauk SSSR, Neorganicheskie Materialy, 1990 , vol. 26, p. 97 - 101
Breederveld, H.; Waterman, H. I.
Research (London), 1952 , vol. 5, p. 537 - 539
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Gmelin Handbook: Si: MVol.C, 149, page 408 - 409
co-catalyst: pyrimidine or P(OPh)3; tri-n-butyl-tin hydride in toluene absence of air; H2-stream; further alternate co-catalysts: PCy3 or PBu3 or N-methylimidazole or pyridine or chinoline; gas chromy.;
参考文献
General Electric Co.
Patent: GB609134 , 1948 ;
C. A., 1950 , p. 6090
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General Electric Co.
Patent: US2406605 , 1946 ;
C. A., 1946 , p. 7236
co-catalyst: Bu3N or TMEDA or DABCO or PhNMe2; tri-n-butyl-tin hydride in toluene absence of air; H2-stream; further alternate co-catalysts: PCy3 or PBu3; gas chromy.;
参考文献
Paetzold; Roewer; Herzog
Journal of Organometallic Chemistry, 1996 , vol. 508, # 1-2 p. 147 - 152
co-catalyst: P(O(i)Pr)3 or PMe2Ph or PPh3; tri-n-butyl-tin hydride in toluene absence of air; H2-stream; further alternate co-catalysts: PCy3 or PBu3 or N-methylimidazole or pyridine or chinoline; gas chromy.;
参考文献
Paetzold; Roewer; Herzog
Journal of Organometallic Chemistry, 1996 , vol. 508, # 1-2 p. 147 - 152