Vol'nov, Yu. N.
Zhurnal obshchei Khim. (russ.), 1939 , vol. 9, p. 2269 - 2282
C. I, 1940 , p. 2307
Full Text Show Details
Gmelin Handbook: Si: MVol.C, 131, page 363 - 365
in neat (no solvent) under inert atmosphere; eqimolar amt. of SiCl4 and SiBr4 equilibrated by stirring at room temp. for 3 d; sepd. by repeated fractional distn. at ambient pressure; immediately frozen; characterized by (29)Si NMR;
参考文献
Hcnsen, Karl; Mayr-Stein, Ralf; Stumpf, Thorsten; Pickel, Peter; Boite, Michael; Fleischer, Holger
Journal of the Chemical Society, Dalton Transactions, 2000 , # 4 p. 473 - 477
in gas High Pressure; reagents added to tube in dry ice bath, sealed in amts. to develop about 30-50 atm of pressure at 300°C, heated at 3o0°C for 17 h; analyzed by GLC;
参考文献
Scaduto, Patricia M.; Speier, John L.
Inorganic Chemistry, 1983 , vol. 22, p. 3363 - 3364
in gas High Pressure; reagents added to tube in dry ice bath, sealed in amts. to develop about 30-50 atm of pressure at 300°C, heated at 310°C for 21-115 h; analyzed by GLC;
参考文献
Scaduto, Patricia M.; Speier, John L.
Inorganic Chemistry, 1983 , vol. 22, p. 3363 - 3364
