in gas High Pressure; reagents added to tube in dry ice bath, sealed in amts. to develop about 30-50 atm of pressure at 300°C, heated at 310-350°C for 1.5-69 h; analyzed by GLC;
参考文献
Scaduto, Patricia M.; Speier, John L.
Inorganic Chemistry, 1983 , vol. 22, p. 3363 - 3364
in gas High Pressure; reagents added to tube in dry ice bath, sealed in amts. to develop about 30-50 atm of pressure at 300°C, heated at 350°C for 65 h; analyzed by GLC;
参考文献
Scaduto, Patricia M.; Speier, John L.
Inorganic Chemistry, 1983 , vol. 22, p. 3363 - 3364
in neat (no solvent) quiet electric discharges on a H2 stream with the mixture of SiCl4- and Br2-vapors, passed through a discharge tube;; mixture obtained;;
in neat (no solvent) passing SiCl4 vapors with HI through a glass tube at red heat;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 611 - 614
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Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
