in gas High Pressure; reagents added to tube in dry ice bath, sealed in amts. to develop about 30-50 atm of pressure at 300°C, heated at 350°C for 65 h; analyzed by GLC;
参考文献
Scaduto, Patricia M.; Speier, John L.
Inorganic Chemistry, 1983 , vol. 22, p. 3363 - 3364
in gas High Pressure; reagents added to tube in dry ice bath, sealed in amts. to develop about 30-50 atm of pressure at 300°C, heated at 3o0°C for 17 h; analyzed by GLC;
参考文献
Scaduto, Patricia M.; Speier, John L.
Inorganic Chemistry, 1983 , vol. 22, p. 3363 - 3364
Gmelin Handbook: U: SVol.C8, 5.1.2, page 12 - 55
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Katz, J. J.; Rabinowitch, E.
The Chemistry of Uranium, Tl.1, McGraw-Hill, New York - Toronto - London 1951, S.355/82
byproducts: Cl, SiO2; on heating UO3 with SiCl4 for 8 h at 370 up to 380 °C in a sealed tube, chlorine forms together with a residue, that contains unchanged UO3, UCl4, UO2Cl2, and SiO2;;
