反应条件
in water High Pressure; addn. of a soln. of NaOH to a soln. of ZrCl4 with strong agitation, pH 6 of the suspn., pptn.; washing (distd. H2O) until Cl(1-) is absent, autoclave treatment (constant pH), filtration, drying (293 K), hydrothermal treatment (6 h at 470 K, 6 h at 570 K, 6-25 h at 670 K), pptn., calcination at 470 and 670 K, drying (370 K); x-ray diffraction;
参考文献
Chertov, V. M.; Kaganovskii, V. A.; Okopnaya, N. T.
Inorganic Materials (Transl. of Neorg. Mater.), 1985 , vol. 21, p. 219 - 223
Izvestiya Akademii Nauk SSSR, Neorganicheskie Materialy, 1985 , vol. 21, p. 269 - 272
