ethanol in ethanol
stirring (ambient temp., Ar atmosphere);
参考文献
Geetha, C. N.; Rani, Indra; Singh, H. B.; Multani, R. K.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1985 , vol. 24, # 3 p. 236 - 237
in dichloromethane
(vac. or Ar atmosphere) dropwise addn. of soln. of (Me3Si)2S (-30°C) to suspn. of metal compound (-78°C), stirring, warming to room temp.; high yield;
参考文献
Gibson, Vernon C.; Shaw, Alan; Williams, David N.
Polyhedron, 1989 , vol. 8, p. 549 - 550
