反应条件
in neat (no solvent) molar ratio niobium ditelluride/PCl5 1/8; heated in evacuated sealed ampoules for 2 h at 170°C, cooled; PCl3 removed in a vac. at 80°C, extd. with hot monoglyme, the residue dried in a vac.; NMR, mass spectra;
参考文献
Sheer, M.; Fedin, V. P.; Fedorov, V. E.; Fedotov, M. A.; Semyannikov, P. P.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1987 , vol. 32, p. 1049 - 1051
Zhurnal Neorganicheskoi Khimii, 1987 , vol. 32, p. 1769 - 1771
