1002754-03-1合成路线 （共 12 条）
反应条件
Multi-step reaction with 6 steps 1: DMAP / CH2Cl2 / -78 °C2: Pd2(DBA)3*CHCl3; triphenylphosphine / CH2Cl2 / 0 - 20 °C3: NaBH4 / CH2Cl2; methanol / -78 °C4: pyridine; DMAP / CH2Cl2 / 20 °C5: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C6: TBAF / tetrahydrofuran / 20 °C
参考文献
Guo, Haibing; O'Doherty, George A. Organic Letters, 2006 , vol. 8, # 8 p. 1609 - 1612
反应条件
Multi-step reaction with 7 steps 1: DMAP / CH2Cl2 / -78 °C2: Pd2(DBA)3*CHCl3; triphenylphosphine / CH2Cl2 / 0 - 20 °C3: NaBH4 / CH2Cl2; methanol / -78 °C4: pyridine; DMAP / CH2Cl2 / 20 °C5: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C6: TBAF / tetrahydrofuran / 20 °C7: triethylamine / CH2Cl2
参考文献
Guo, Haibing; O'Doherty, George A. Organic Letters, 2006 , vol. 8, # 8 p. 1609 - 1612
