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乙二醇
甲醛
63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴噻吩
合成路线
（共 523 条）
1003-09-4
2-溴噻吩
+
100-63-0
苯肼
→
反应条件
825-55-8
2-苯基噻吩
+
92-52-4
联苯
+
492-97-7
2,2'-联二噻吩
反应条件
sodium hydroxide; mercury dichloride; palladium dichloride in methanol 6 h; Heating; Title compound not separated from byproducts;
参考文献
Nakajima; Kinosada; Tamura; Hara
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 4 p. 1113 - 1115
1003-09-4
2-溴噻吩
+
13294-71-8
2-溴-2-丁烯
→
反应条件
100005-76-3
+
1187-40-2
+
492-97-7
2,2'-联二噻吩
反应条件
NiBr2bipy in N,N-dimethyl-formamide Ambient temperatureelectrolysis; nickel-sponge cathode, aluminium rod anode, NBu4BF4 supporting electrolyte; current intensity 0.15 to 0.2 A; Yield given;
参考文献
Durandetti, Muriel; Perichon, Jacques; Nedelec, Jean-Yves
Tetrahedron Letters, 1997 , vol. 38, # 50 p. 8683 - 8686
1003-09-4
2-溴噻吩
+
98-80-6
苯硼酸
→
反应条件
825-55-8
2-苯基噻吩
+
492-97-7
2,2'-联二噻吩
反应条件
triethylamine; polystyrene-b-poly(rhodium acrylate)-Pd nanoparticles in water; acetonitrile Suzuki coupling; 24 h; Product distribution; Further Variations:CatalystsSolvents;
参考文献
Li, Yin; El-Sayed, Mostafa A.
Journal of Physical Chemistry B, 2001 , vol. 105, # 37 p. 8938 - 8943
1003-09-4
2-溴噻吩
→
反应条件
163928-54-9
+
492-97-7
2,2'-联二噻吩
+
144852-97-1
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Effenberger, Franz; Wuerthner, Frank; Steybe, Felix
Journal of Organic Chemistry, 1995 , vol. 60, # 7 p. 2082 - 2091
110-86-1
吡啶
+
1003-09-4
2-溴噻吩
→
反应条件
492-97-7
2,2'-联二噻吩
+
3480-11-3
5-溴-2,2′-联噻吩
+
82080-27-1
+
3319-99-1
反应条件
trans-lt;Mo(N2)2(Ph2PCH2CH2PPh2)2gt; 4 h; Irradiation; Product distribution;
参考文献
Minzoni, Ferruccio; Nardelli, Mario; Pelizzi, Corrado; Predieri, Giovanni
Gazzetta Chimica Italiana, 1984 , vol. 114, # 5/6 p. 221 - 224
1003-09-4
2-溴噻吩
→
反应条件
188290-36-0
+
2404-89-9
+
34557-54-5
+
492-97-7
2,2'-联二噻吩
反应条件
PyrolysisIR laser powering; Product distribution; Further Variations:Reagents;
参考文献
Hore, Nathan R.; Russell, Douglas K.
New Journal of Chemistry, 2004 , vol. 28, # 5 p. 606 - 613
1003-09-4
2-溴噻吩
+
30418-59-8
→
反应条件
92057-12-0
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in ethanol; toluene T=60°C; Suzuki Coupling; 12 h; Inert atmosphere;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 23 p. 7268 - 7271
1003-09-4
2-溴噻吩
+
115-19-5
→
反应条件
4298-52-6
反应条件
potassium hydroxide; diethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide 2.) MeOH, reflux; Multistep reaction;
参考文献
Novak, Igor; Ng, Siu Choon; Fang, Jiye; Mok, Chup Yew; Huang, Hsing Hua
Journal of Physical Chemistry, 1994 , vol. 98, # 3 p. 748 - 751
1003-09-4
2-溴噻吩
+
5720-07-0
→
反应条件
42545-43-7
反应条件
potassium phosphate; tetrabutylammomium bromide; palladium diacetate in ethanol T=20°C; Suzuki cross-coupling reaction; 3 h;
参考文献
Deng, Yijian; Gong, Liuzhu; Mi, Aiqiao; Liu, Hui; Jiang, Yaozhong
Synthesis, 2003 , # 3 p. 337 - 339
1003-09-4
2-溴噻吩
+
696-62-8
→
反应条件
42545-43-7
反应条件
PEG 4000; palladium diacetate; potassium carbonate T=120°C; 10 h;
参考文献
Wang, Liang; Zhang, Yuhong; Liu, Leifang; Wang, Yanguang
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1284 - 1287
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