in acetonitrile T=35°C; 0.5 h; Irradiationother halothiophenes; var. reaction time, also in presence electron acceptors; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 52, # 24 p. 5382 - 5386
1: thien-2-yl bromide With magnesium in tetrahydrofuran 0.75 h; Inert atmosphereReflux; 2: carbon dioxide in tetrahydrofuran T=-78 - 20°C;
参考文献
Van De Kruijs, Bastiaan H. P.; Dressen, Mark H. C. L.; Meuldijk, Jan; Vekemans, Jef A. J. M.; Hulshof, Lumbertus A.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 7 p. 1688 - 1694