Battersby, Alan R.; Dutton, Christopher J.; Fookes, Christopher J. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1569 - 1576
Battersby, Alan R.; Dutton, Christopher J.; Fookes, Christopher J. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1569 - 1576
in toluene
Ar atmosphere, stirring (60°C, 3 h); solvent removal (14 Torr), B-product isolated by sublimation (30-40°C, 0.001 Torr); byproducts identified by MS and (31)P-NMR;