(S)-(-)-3-氯-1-苯基-1-丙醇合成路线 (共 28 条)
反应条件
potassium formiate; Cp*IrCl[(S,S)-MsDPEN] in water; toluene T=50°C; 24 h; Product distribution / selectivity;
参考文献
Zhou, Ji-Ning; Fang, Qiang; Hu, Yi-Hu; Yang, Li-Yao; Wu, Fei-Fei; Xie, Lin-Jie; Wu, Jing; Li, Shijun
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 6 p. 1009 - 1017
反应条件
dimethylsulfide borane complex; (+)-3-exo-amino-7,7-dimethoxynorbornan-2-exo-ol in tetrahydrofuran T=25°C; 2 h;
参考文献
Lapis, Alexandre A. M.; De Fatima, Angelo; Martins, Jose E. D.; Costa, Valentim E. U.; Pilli, Ronaldo A.
Tetrahedron Letters, 2005 , vol. 46, # 3 p. 495 - 498
反应条件
in ethanol T=20°C; 16 h; bakers' yeast in aq. glucose solution;
参考文献
Journal of Organic Chemistry, , vol. 56, # 21 p. 6019 - 6023
反应条件
Pseudomonas cepacia lipase immobilized on toyonite; potassium tert-butylate; sodium carbonate; [2,3,4,5-Ph4(η5-C4CNH(i-Pr))]Ru(CO)2Cl in toluene T=25°C; 168 h;
参考文献
Choi, Jun Ho; Choi, Yoon Kyung; Kim, Yu Hwan; Park, Eun Sil; Kim, Eun Jung; Kim, Mahn-Joo; Park, Jaiwook
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1972 - 1977
反应条件
yeast strain Aureobasidium pullulans CQA T=28°C; 48 h; Microbiological reactionEnzymatic reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 102, p. 94 - 98
反应条件
methanol; potassium carbonate
参考文献
Schneider; Goergens
Tetrahedron Asymmetry, 1992 , vol. 3, # 4 p. 525 - 528
反应条件
novozyme 435 in hexane T=30°C; Esterification; Resolution of racemate; 192 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 11 p. 1767 - 1769
反应条件
Bacillus subtilis esterase in ethanol T=30°C; pH=7.2; 12 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 3 p. 405 - 414
反应条件
lipase from Pseudomonas fluorescens in hexane T=20°C; 82 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Pop, Laura Ancua; Czompa, Andrea; Paizs, Csaba; Toa, Monica Ioana; Vass, Elemer; Matyus, Peter; Irimie, Florin-Dan
Synthesis, 2011 , # 18 art. no. T49711SS, p. 2921 - 2928