4-苄氨基-3-硝基吡啶合成路线 （共 11 条）
反应条件
triethylamine in dichloromethane 18 h; Reflux;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 38 p. 6526 - 6545
反应条件
in methanol; benzylamine
参考文献
US5571819 A1, ;
US 5571819 A
反应条件
in isopropyl alcohol T=20°C; 24 h; Inert atmosphere;
参考文献
Organic Process Research and Development, , vol. 12, # 6 p. 1261 - 1264
反应条件
1: 70 percent / fuming HNO3, fuming H2SO4 / 1,2-dichloro-ethane / 7 h / 80 - 82 °C 2: PCl5 / 1) PCl5, 1,2-dichloroethane, reflux, 6 h , 2) reflux, 1 h 3: 163 g / ethanol / 18 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 23, # 3 p. 669 - 672
反应条件
1: PCl5 / 1) PCl5, 1,2-dichloroethane, reflux, 6 h , 2) reflux, 1 h 2: 163 g / ethanol / 18 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 23, # 3 p. 669 - 672
反应条件
in acetonitrile T=60°C; 24 h; Inert atmosphere;
参考文献
Organic Process Research and Development, , vol. 12, # 6 p. 1261 - 1264
反应条件
in ethanol 18 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 23, # 3 p. 669 - 672
反应条件
hydrogen; palladium on activated charcoal in ethanol T=80°C; P=3102.9 Torr; 30 h;
参考文献
Campbell; Greene; Lavagnino; et al.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 3 p. 669 - 672
反应条件
ammonia in methanol; ethanol; water
参考文献
US5571819 A1, ;
US 5571819 A
