反应条件
benzene in neat (no solvent) homogenizing of CrBr3, Al and AlBr3 (N2 atmosphere), benzene addn., stirring (room temp., 14 h), solvolysis (H2O/MeOH/petroleum ether, ice cooling), water/methanolic phase redn. (Na2S2O4/KOH/benzene); benzene phase sepn., drying (KOH), evapn., recrystn. (THF, -80°C), sublimation;
参考文献
Elschenbroich, Christoph; Moeckel, Reinhart; Zenneck, Ulrich; Clack, Denis W.
Berichte der Bunsen-Gesellschaft fuer Physikalische Chemie, 1979 , vol. 83, p. 1008 - 1018
