反应条件
Multi-step reaction with 6 steps 1: 74 percent / K2CO3 / dimethylformamide / 1 h / Heating2: 88 percent / POCl3 / CH2Cl2 / Ambient temperature3: 90 percent / Zn-amalgam, 4 N aq. HCl / dioxane / 2 h / Heating4: H2 / 10percent Pd/C / ethyl acetate / 0.25 h / Ambient temperature5: pyridine / 2 h / Heating6: 68 percent / CrO3, water / acetic acid / 4 h / Ambient temperature
参考文献
Pillai; Naiksatam; Johnson; et al. Journal of Organic Chemistry, 1986 , vol. 51, # 5 p. 717 - 723