1,3,4,6-四-O-乙酰基-2-氨基-alpha-D-吡喃葡萄糖盐酸盐合成路线 (共 26 条)
反应条件
With 4-(N,N-dimethlyamino)pyridine in dichloromethane 2 h; Show Experimental Procedure
参考文献
SIMON FRASER UNIVERSITY Patent: WO2008/25170 A1, 2008 ; Location in patent: Page/Page column 61-62 ;WO 2008/025170 A1
反应条件
With hydrogenchloride in acetone Heating;
参考文献
Cunha; Pereira; De Souza; Ferreira Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 8 p. 1555 - 1569
反应条件
Multi-step reaction with 3 steps 1: 97 percent / aq. NaOH / 4 °C2: 72 percent / pyridine / 20 °C3: 100 percent / HCl / acetone
参考文献
Kyas, Andreas; Feigel, Martin Helvetica Chimica Acta, 2005 , vol. 88, # 9 p. 2375 - 2396
反应条件
With triethylamine Show Experimental Procedure
参考文献
UNIVERSITY OF GEORGIA RESEARCH FOUNDATION, INC. Patent: US2008/20997 A1, 2008 ; Location in patent: Page/Page column Sheet 4/17; Sheet 6/17; 11 ;
反应条件
Multi-step reaction with 2 steps 1: 1. NaHCO3 / 1. H2O 2. CHCl3, 1 h, room temperature2: 33percent HBr / acetic acid / 3 h / Ambient temperature
参考文献
Boullanger, Paul; Jouineau, Martine; Bouammali, Boufelja; Lafont, Dominique; Descotes, Gerard Carbohydrate Research, 1990 , vol. 202, p. 151 - 164
反应条件
Multi-step reaction with 2 steps 1: K2CO3 / dimethylformamide2: N2O4, NaOAc / CH2Cl2 / 0.08 h
参考文献
Dasgupta, Falguni; Garegg, Per J. Journal of the Chemical Society, Chemical Communications, 1989 , # 21 p. 1640 - 1641