反应条件
in water passing PH3 (prepared from Ca-phosphide and HCl) into an aq. suspension of I2 in a bulb under CO2 or N2 (agitation) until initial brown discoloration has vanished;; removal of H2O and HI by repeated distn. at 40 °C and 40 Torr and addn. of small amounts of water to the residue before 2nd and 3rd distillation;;
参考文献
P: MVol.C, 46, page 93 - 95
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 223, p. 242 - 243
