Gredy
Bulletin de la Societe Chimique de France, 1935 , vol. <5> 2, p. 1029,1033
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1936 , vol. 202, p. 664
in ethanol
concd. HBr added to a soln. of Sn-compound in EtOH; mixture stirred at room temp. for 2 h; volatiles removed under vacuum; recrystallized from CHCl3;
参考文献
Howie, R. Alan; Moura, Marcelo V.H.; Wardell, James L.; Wardell, Solange M.S.V.
Polyhedron, 2004 , vol. 23, # 14 p. 2331 - 2336
aluminum tribromide in benzene
N2-atmosphere; saturation of soln. of silane-AlBr3 with HBr for 1 h; evapn., addn. of heptane, filtration, evapn., not sepd.; NMR spectroscopy;
参考文献
Poeschl, Ulrich; Hassler, Karl
Organometallics, 1996 , vol. 15, # 14 p. 3238 - 3240
