in neat (no solvent) byproducts: benzene; HBr condenced onto layer of phenylgermane at liquid N2 temp.; react. mixt sealed in Pyrex vessel and slowly heated overnight to room temp.; resulting mixt. pyrified by trap-to-trap distn. in vac.; gas phase IR;
参考文献
Tackett, Brandon S.; Li, Yunjing; Clouthier, Dennis J.; Pacheco, Kezia L.; Schick, G. Alan; Judge, Richard H.
Journal of Chemical Physics, 2006 , vol. 125, # 11 art. no. 114301