2-乙酰氨基-2-脱氧-Alpha-D-吡喃糖合成路线 （共 58 条）
反应条件
bovine kidney α-fucosidase; jack bean β-N-acetylhexosaminidase T=37°C; pH=5; 24 h; aq. bufferEnzymatic reaction;
参考文献
Glycobiology, , vol. 20, # 8 art. no. CWQ064, p. 1021 - 1033
反应条件
bovine kidney α-fucosidase; jack bean β-N-acetylhexosaminidase T=37°C; pH=5; 24 h; aq. bufferEnzymatic reaction;
参考文献
Glycobiology, , vol. 20, # 8 art. no. CWQ064, p. 1021 - 1033
反应条件
1.1: sodium methylate / methanol / 2 h / 20 °C 1.2: Amberlite IR-120 (H+ form) 2.1: Jack bean N-acetyl-β-D-glucosaminidase / isopropyl alcohol / 48 h / 37 °C / pH 5 / aq. sodium phosphate buffer; Enzymatic reaction View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 19 p. 6949 - 6955
反应条件
1.1: acetonitrile / 0.17 h / 20 °C / Molecular sieve 1.2: 25 h / 55 - 80 °C 2.1: sodium methylate / methanol / 2 h / 20 °C 2.2: Amberlite IR-120 (H+ form) 3.1: Jack bean N-acetyl-β-D-glucosaminidase / isopropyl alcohol / 48 h / 37 °C / pH 5 / aq. sodium phosphate buffer; Enzymatic reaction View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 19 p. 6949 - 6955
反应条件
phosphate buffer T=30°C; 52 h; β-N-acetylhexosaminidase from Aspergillus oryzae; Further byproducts given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 6, # 11 p. 2803 - 2810
反应条件
phosphate buffer T=30°C; 52 h; β-N-acetylhexosaminidase from Aspergillus oryzae; Further byproducts given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 6, # 11 p. 2803 - 2810
反应条件
Amberlite IRA-68 (HO-); acetic acid 1.) MeOH, water, 24 h, RT; 2.) 24 h, RT; 3.) ether, 60 min, 60 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 175, p. 311 - 316
反应条件
citrate-phosphate buffer; β-N-acetylhexosaminidase from Aspergillus oryzae CCF 1066 T=37°C; pH=5.0; 3 h; Enzymatic reaction; Product distribution; Further Variations:Reagents;
参考文献
Advanced Synthesis and Catalysis, , vol. 345, # 6-7 p. 735 - 742
反应条件
chitinase from Streptomyces griseus in phosphate buffer T=30°C; Deacetylation; pH=6.0; 1 h; Enzymatic reaction; Product distribution;
参考文献
Carbohydrate Research, , vol. 316, # 1-4 p. 173 - 178
反应条件
sodium hydrogencarbonate; hydrazine 1.) 100 deg, 24 h, 2.) r.t., 1 h. 2-acetamido-1-N-(L-aspart-4-oyl)-2-deoxy-β-D-gluopyranosylamine was used as model glycopeptide to study hydrazinolysis-N-reacylation procedure.;
参考文献
Carbohydrate research, , vol. 144, # 1 p. 1 - 12
