2-乙酰氨基-2-脱氧-Alpha-D-吡喃糖合成路线 （共 58 条）
反应条件
boron trifluoride diethyl etherate T=90°C; 5 h;
参考文献
ISIS INNOVATION LIMITED
Patent: WO2007/93769 A1, 2007 ;
Location in patent: Page/Page column 24; 28-29 ;
反应条件
1: 75 percent / acetyl chloride / 0 - 70 °C 2: 77 percent / pyridine / CH2Cl2 / -60 °C 3: 96 percent / NaN3; NaI / acetonitrile / 48 h / 60 °C 4: pyridine / CH2Cl2 / 1 h / -15 °C 5: 3.07 g / dimethylformamide / 20 h / 20 °C 6: sodium methoxide / methanol / 3 h / 20 °C / pH 9.0 View Scheme
参考文献
Roy, Rene; Kim, Jin Mi
Tetrahedron, 2003 , vol. 59, # 22 p. 3881 - 3893
反应条件
recombinant galactokinase from Streptococcus pneumoniae TIGR4; magnesium chloride T=45°C; pH=8; 3 h; aq. bufferEnzymatic reaction;
参考文献
Chen, Min; Chen, Lei-Lei; Zou, Yang; Xue, Mengyang; Liang, Min; Jin, Lan; Guan, Wan-Yi; Shen, Jie; Wang, Wenjun; Wang, Lei; Liu, Jun; Wang, Peng George
Carbohydrate Research, 2011 , vol. 346, # 15 p. 2421 - 2425
反应条件
Yield given. Multistep reaction;
参考文献
Nicolaou K. C.; Hummel, C. W.; Bockovich, N. J.; Wong, C. H.
Journal of the Chemical Society, Chemical Communications, 1991 , # 13 p. 870 - 872
反应条件
pyridine 1) 4 d, RT; 2) 0 deg C, then 48 h, RT; Yield given. Multistep reaction;
参考文献
Timoshchuk, V. A.; Kulinkovich, L. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 4 p. 919 - 922,815 - 818
反应条件
toluene-4-sulfonic acid in toluene 3 h; Reflux;
参考文献
Babic, Andrej; Pecar, Slavko
Tetrahedron Asymmetry, 2008 , vol. 19, # 19 p. 2265 - 2271
反应条件
amberlite IR120(H) 16 h; Heating / reflux;
参考文献
McGill University
Patent: US2006/211634 A1, 2006 ;
Location in patent: Page/Page column 17 ;
反应条件
toluene-4-sulfonic acid 24 h; Heating;
参考文献
Kida, Toshiyuki; Yurugi, Keiji; Masuyama, Araki; Nakatsuji, Yohji; Ono, Daisuke; Takeda, Tokuji
Journal of the American Oil Chemists' Society, 1995 , vol. 72, # 7 p. 773 - 780
