8-(5-己基-2-呋喃基)-辛酸甲酯合成路线 （共 11 条）
反应条件
trifluoroacetic acid in 1,2-dichloro-ethane
T=60°C; 3 h;
参考文献
Jie, Marcel S. F. Lie Ken; Zheng, Y. F.
Synthesis, 1988 , # 6 p. 467 - 468
反应条件
boron trichloride in methanol
0.5 h; Heating;
参考文献
Khan, Mushfiquddin; Hashmi, Mazzaz; Ahmad, Fasih; Osman, S. M.
Journal of the Chemical Society, Chemical Communications, 1983 , # 19 p. 1057 - 1058
反应条件
N,N-dimethyl-thioformamide; trifluoroacetic acid in 1,2-dichloro-ethane
T=60°C; 3 h;
参考文献
Jie, Marcel S. F. Lie Ken; Zheng, Y. F.
Synthesis, 1988 , # 6 p. 467 - 468
反应条件
1: chromic acid / diethyl ether
2: 46 percent / Zn filings, di-iodomethane / 1,2-dimethoxy-ethane / 4 h / 80 - 90 °C / Irradiation; ultrasound; different metal filings
View Scheme
参考文献
Lie, Marcel S. F.; Jie, Ken; Lam, Wilson L. K.
Journal of the Chemical Society, Chemical Communications, 1987 , # 19 p. 1460 - 1461
反应条件
1: 82.6 percent / pyridinium chlorochromate, AcONa / CH2Cl2
2: 100 percent / aq. ethylmethyldioxirane / butan-2-one / 1 h
3: TiCl4 / CH2Cl2; tetrahydrofuran / 1.5 h / Ambient temperature
View Scheme
参考文献
Foglia; Sonnet; Nunez; Dudley
JAOCS, Journal of the American Oil Chemists' Society, 1998 , vol. 75, # 5 p. 601 - 607
反应条件
1: m-chloroperbenzoic acid
2: NaI, nPrI / dimethylsulfoxide
View Scheme
参考文献
Jie, Marcel S. F. Lie Ken; Ahmad, Fasih
Journal of the Chemical Society, Chemical Communications, 1981 , # 21 p. 1110 - 1111
反应条件
1: 560 mg / oxygen, Methylene Blue / CCl4; methanol / 16 h / Irradiation
2: 50 percent / ferrous sulphate / H2O; tetrahydrofuran / 5 h / Ambient temperature
View Scheme
参考文献
Bascetta, Emanuele; Gunstone, Frank D.; Scrimgeour, Charles M. S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2199 - 2206
反应条件
1: 4.7 g / pyridine / 1.) 0 deg C, 2 h, 2.) 5-10 deg C, 2 h
2: 1,8-diazabicyclo<5.4.0>undec-7-ene / toluene / 4 h / Heating
3: 560 mg / oxygen, Methylene Blue / CCl4; methanol / 16 h / Irradiation
4: 50 percent / ferrous sulphate / H2O; tetrahydrofuran / 5 h / Ambient temperature
View Scheme
参考文献
Bascetta, Emanuele; Gunstone, Frank D.; Scrimgeour, Charles M. S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2199 - 2206
反应条件
1: 1,8-diazabicyclo<5.4.0>undec-7-ene / toluene / 4 h / Heating
2: 560 mg / oxygen, Methylene Blue / CCl4; methanol / 16 h / Irradiation
3: 50 percent / ferrous sulphate / H2O; tetrahydrofuran / 5 h / Ambient temperature
View Scheme
参考文献
Bascetta, Emanuele; Gunstone, Frank D.; Scrimgeour, Charles M. S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2199 - 2206
反应条件
1-iodo-propane; sodium iodide in dimethyl sulfoxide
Title compound not separated from byproducts;
参考文献
Jie, Marcel S. F. Lie Ken; Ahmad, Fasih
Journal of the Chemical Society, Chemical Communications, 1981 , # 21 p. 1110 - 1111
