反应条件
in neat (no solvent)
Ar atmosphere; addn. excess of 1,4-dioxane to mixt. of HGeCl3 and GeCl4 (stirring), pptn.; removal of excess of dioxane, GeCl4 Vac.), drying (vac.);
参考文献
Mont, Wolf-W. du; Lange, Lutz; Pohl, Siegfried; Saak, Wolfgang
Organometallics, 1990 , vol. 9, p. 1395 - 1399