2-甲氧基-5,5-二甲基-1,3,2-二氧磷杂环己烷合成路线 （共 26 条）
反应条件
trimethylsilyl bromide
T=80°C; Inert atmosphere;
参考文献
Dabkowski, Wojciech; Ozarek, Alfred; Olejniczak, Sebastian; Cypryk, Marek; Chojnowski, Julian; Michalski, Jan
Chemistry - A European Journal, 2009 , vol. 15, # 7 p. 1747 - 1756
参考文献
Patois, Carl; Ricard, Louis; Savignac, Philippe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 6 p. 1577 - 1581
反应条件
stirred at 20 deg C, causing an exothermic reaction, tepm. rose to 120 deg C;
参考文献
Morita, Iwao; Tsuda, Masami; Kise, Masahiro; Sugiyama, Makoto
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 12 p. 4711 - 4716
反应条件
trimethylamine-N-oxide in acetone; acetonitrile
T=60°C;
参考文献
Brault,J.-F.; Chabrier,P.
Bulletin de la Societe Chimique de France, 1974 , p. 677 - 680
反应条件
in acetone; acetonitrile
T=60°C;
参考文献
Chabrier,P.; Brault,J.-F.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1973 , vol. 276, p. 1135 - 1137
反应条件
1: 63 percent
2: 52 percent / benzene
3: pyridine
View Scheme
参考文献
Baraniak; Stec
Tetrahedron Letters, 1991 , vol. 32, # 1 p. 137 - 140
