1: With 4 A molecular sieve; quinine-based catalyst in toluene
T=50°C; oxy-Michael addition; 37 h;
2: With dihydrogen peroxide; sodium carbonate in ethyl acetate; toluene
T=20°C; 0.25 h; Further stages. Title compound not separated from byproducts.;
参考文献
De, Run Li; Murugan, Andiappan; Falck
Journal of the American Chemical Society, 2008 , vol. 130, # 1 p. 46 - 48