8-Exo-碘-2-氮杂双环[3.3.0]-3-辛酮合成路线 （共 5 条）
反应条件
iodine in tetrahydrofuran 0.166667 h; Yield given;
参考文献
Knapp, Spencer; Levorse, Anthony T.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4006 - 4014
反应条件
1: oxalyl chloride / toluene / 1.5 h 2: liq. NH3 3: triethylamine / pentane / 0.5 h / 23 °C 4: I2 / tetrahydrofuran / 0.17 h View Scheme
参考文献
Knapp, Spencer; Levorse, Anthony T.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4006 - 4014
反应条件
1: liq. NH3 2: triethylamine / pentane / 0.5 h / 23 °C 3: I2 / tetrahydrofuran / 0.17 h View Scheme
参考文献
Knapp, Spencer; Levorse, Anthony T.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4006 - 4014
反应条件
1: triethylamine / pentane / 0.5 h / 23 °C 2: I2 / tetrahydrofuran / 0.17 h View Scheme
参考文献
Knapp, Spencer; Levorse, Anthony T.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4006 - 4014
反应条件
pyridine; water; silver trifluoroacetate
1.) nitromethane, 2.) 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Knapp, Spencer; Levorse, Anthony T.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4006 - 4014
